1. Leaking rubber gasket. I had an intake plenum gasket make that noise before. Check the tightness of all plenum bolts, especially if you used Fel-Pro gaskets (they have a small rubber seal that can vibrate if leaking making the noise).
I am in no way doubting....just never heard a PVC valve whistle....guess it could...guess Ive never had one go that bad.....learn something new everyday